CHEMICAL HYGIENE PLAN

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Department of Chemical Engineering
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2. Standard Operating Procedures

A. Use of "Prudent Practices in the Laboratory: Handling and Disposal of Chemicals"

Laboratory operating procedures found in "Prudent Practices in the Laboratory: Handling and Disposal of Chemicals" (National Research Council, 1995) are adopted for general use at the University of Minnesota. The table of contents and Chapter 1 "The Culture of Laboratory Safety", Chapter 5 "Working with Chemicals" and Chapter 6 "Working with Laboratory Equipment" are reproduced in Appendix D and can be accessed by University of Minnesota Personnel electronically from DEHS's web site (www.dehs.umn.edu). The following topics are covered in Chapters 5 and 6 of Prudent Practices:

Chapter 5: Working with Chemicals

  • Introduction
  • Prudent Planning
  • General Procedures for Working with Hazardous Chemicals
  • Working with Substances of High Toxicity
  • Working with Biohazardous and Radioactive Materials
  • Working with Flammable Chemicals
  • Working with Highly Reactive or Explosive Chemicals
  • Working with Compressed Gases


Chapter 6: Working with Laboratory Equipment

  • Introduction
  • Working with Water-Cooled Equipment
  • Working with Electrically Powered Laboratory Equipment
  • Working with Compressed Gases
  • Working with High/Low Pressures and Temperatures
  • Using Personal Protective, Safety, and Emergency Equipment
  • Emergency Procedures


B. Other References

The American Chemical Society's "Safety in Academic Chemistry Laboratories" is another useful text. This manual presents information similar to that found in Prudent Practices, but in a considerably condensed format.

C. University of Minnesota Standards and Recommended Practices

Selected standard operating procedures have been adopted by the University of Minnesota specifically for its own laboratories. Extensive and detailed policies regarding hazardous waste management are specified in the University's guide book "Hazardous Chemical Waste Management, 5th edition." During a chemical spill in the laboratory, workers should follow Part 3: Emergency Procedures of this guide book.

The "Quick Reference" from this section is reproduced below.

Quick Reference

Chemical Spill Emergency Procedures

Evacuate
  • Leave the spill area; alert others in the area and direct/assist them in leaving.
  • Without endangering yourself: remove victims to fresh air, remove contaminated clothing and flush contaminated skin and eyes with water for 15 minutes. If anyone has been injured or exposed to toxic chemicals or chemical vapors, call 911 and seek medical attention immediately.


Confine
  • Close doors and isolate area. Prevent people from entering spill area.


Report
  • From a safe place call the UMD Office of Environmental Health and Safety (EHS) Mahjoub Labyad (7232) during working hours, after hours 9-725-6751.
  • Report that this is an emergency and give your name, phone and location; location of the spill; the name and amount of material spilled; extent of injuries; safest route to the spill.
  • Stay by that phone, EHS will advise you as soon as possible.
  • EHS or the Fire Department will clean up or stabilize spills which are considered high hazard (fire, health or reactivity hazard). In the case of a small spill and low hazard situation, EHS will advise you on what precautions and protective equipment to use.


Secure
  • Until emergency response personnel arrive; block off the areas leading to the spill, lock doors, post signs, and warning tape, and alert others of the spill.
  • Post staff by commonly used entrances to the area to direct people to use other routes.


Other more specific standard operating procedures are reproduced in Appendix E.

D. Laboratory Specific Standard Operating Procedures

This section summarizes laboratory specific Standard Operating Procedures (SOPs). The full text of these SOPs is included in Appendix N, or can be obtained from the referenced PI, or from the Laboratory Safety Officer, Duane Long, for the Department of Chemical Engineering. Safety information is included in each SOP, and may be highlighted in a Laboratory Safety Information Sheet, similar to the one included in Appendix F. NOTE: At this time the Department of Chemical Engineering does not have any SOPs




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This web page (http://www.d.umn.edu/~dlong/chp/chplan2.html) is maintained by Duane Long, Department of Chemical Engineering, and was last updated 09-Feb-2001.