SCHEDULE OF EXPERIMENTS

CHEM 2544 - Organic Chemistry II Laboratory Summer 2013

 

 

 

Laboratory handouts can be found at: http://www.d.umn.edu/~pgrundt/2544/Handouts.zip

 

Check-in and safety orientation.

 

Experiment 1:     IR and NMR Spectroscopy, Chapters 11 and 12 - Identification of Unknowns.  

Experiment 2:     Oxidation: Cyclohexanone from Cyclohexanol by Hypochlorite Oxidation, Chapter 22 (Experiment: 5th Edition pp. 381-383; 6th Edition pp. 361-364)

Experiment 3:     Sodium Borohydride Reduction of 2-Methylcyclohexanone, Chapter 26 (Experiment: 5th Edition pp. 419-423; 6th Edition pp. 390-394. In both editions skip Computational Chemistry.)  

Experiment 4:     Aldehydes and Ketones, Chapter 36. Unknowns (Experiments: 1, 2, 3, 6, 7. 5th Edition pp. 502-514; 6th Edition pp. 467-478)  

Experiment 5:     Esterification, Chapter 40. Synthesis of n-Butyl Acetate by Azeotropic Distillation of Water (Experiments 1: 5th Edition pp. 559-560; 6th Edition pp. 520-521)

Experiment 6:     Polymers, Chapter 67 (Experiment 1: 5th Edition pp. 818-820; 6th Edition pp. 763- 764.)

Experiment 7:     Nitration of Methyl Benzoate, Chapter 28. (Experiment 1:  5th Edition pp 432-433; 6th Edition pp 402-403)  

Experiment 8:     Friedel-Crafts Alkylation of Benzene, Chapter 29 (Experiment 1: 5th Edition  pp. 437-440; 6th Edition: pp. 407-410)

Experiment 9:    Amines, Chapter 43 (Experiments: 1 and 2; 5th Edition: 586-590; 6th Edition: 545-548.)

Experiment 10:   The Sandmeyer Reaction, Chapter 44 (Experiments 1, 2, 3: 5th Edition pp 596-601; 6th Edition: pp. 554-559)   

Experiment 11:   Dyes and Dyeing, Chapter 46. Diazotization of Sulfanilic Acid and Preparation of Methyl Orange (Experiments 1, 4: 5th Edition pp. 635-636, 639-640; 6th Edition pp. 592, 596-597.)

Experiment 12:   Carbohydrates, Chapter 63 (Experiments: 2, 3:  5th Edition: pp. 770-771; 6th Edition: pp. 723-724.)

 

Check-out